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Simultaneous analysis of major ingredients of Gardenia fruit by HPLC-MS/TQMS method
http://hdl.handle.net/10258/00009509
http://hdl.handle.net/10258/0000950961b1b2d9-383b-44a7-8673-055ea77366c5
名前 / ファイル | ライセンス | アクション |
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Mong_J_Chem17(43)_34-37 (744.0 kB)
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Item type | 学術雑誌論文 / Journal Article.(1) | |||||||||||
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公開日 | 2018-01-10 | |||||||||||
タイトル | ||||||||||||
言語 | en | |||||||||||
タイトル | Simultaneous analysis of major ingredients of Gardenia fruit by HPLC-MS/TQMS method | |||||||||||
言語 | ||||||||||||
言語 | eng | |||||||||||
キーワード | ||||||||||||
言語 | en | |||||||||||
主題Scheme | Other | |||||||||||
主題 | HPLC-MS/TQMS | |||||||||||
キーワード | ||||||||||||
言語 | en | |||||||||||
主題Scheme | Other | |||||||||||
主題 | geniposide | |||||||||||
キーワード | ||||||||||||
言語 | en | |||||||||||
主題Scheme | Other | |||||||||||
主題 | genipingentiobioside | |||||||||||
キーワード | ||||||||||||
言語 | en | |||||||||||
主題Scheme | Other | |||||||||||
主題 | quantity control | |||||||||||
資源タイプ | ||||||||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||||||||
資源タイプ | journal article | |||||||||||
アクセス権 | ||||||||||||
アクセス権 | open access | |||||||||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||||||||
著者 |
GALAGIN, M
× GALAGIN, M× 上井, 幸司
WEKO
911
× 湯口, 実× 岩佐, 達郎 |
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室蘭工業大学研究者データベースへのリンク | ||||||||||||
上井 幸司(UWAI Koji) | ||||||||||||
http://rdsoran.muroran-it.ac.jp/html/100000240_ja.html | ||||||||||||
室蘭工業大学研究者データベースへのリンク | ||||||||||||
岩佐 達郎(IWASA Tatsuo) | ||||||||||||
http://rdsoran.muroran-it.ac.jp/html/100000119_ja.html | ||||||||||||
抄録 | ||||||||||||
内容記述タイプ | Abstract | |||||||||||
内容記述 | An efficient, accurate HPLC-MS/TQMS method was introduced for the quantitative/qualitative simultaneous analysis of main ingredients, namely geniposide and genipingentiobioside, in the Gardenia fruit. The separation was successfully obtained using a C8 (100mm×2.1mm, 5μm, 30°C) column by gradient elution with ultrapure water as mobile phase, where flow rate was set to 0.2 ml/min and detection wavelength at 240 nm. The analytical method was validated and the quantification of active compounds, namely genipingentiobioside and gardenoside, was performed. Linearity, precision, repeatability, stability and recovery were also reported. The quantitative analysis revealed that both main ingredients as geniposide and genipingentiobioside have performed a good linear relationship in 0.1-100 mg/ml concentration range (r=1.00000 and r =0.99998). The average content was measured to be 4.842% with RSD 0.96% for geniposide and 1.1976% with RSD 0.47% for genipingentiobioside in the Gardenia fruit. Accordingly, this method would be feasible for the quantity and quality control of crude drugs. | |||||||||||
言語 | en | |||||||||||
書誌情報 |
en : Mongolian Journal of Chemistry 巻 17, 号 43, p. 34-37, 発行日 2016-12 |
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出版者 | ||||||||||||
言語 | en | |||||||||||
出版者 | Institute of Chemistry & Chemical Technology Mongolian Academy of Sciences | |||||||||||
出版者版へのリンク | ||||||||||||
10.5564/mjc.v17i43.744 | ||||||||||||
https://dx.doi.org/10.5564/mjc.v17i43.744 | ||||||||||||
DOI | ||||||||||||
関連タイプ | isIdenticalTo | |||||||||||
識別子タイプ | DOI | |||||||||||
関連識別子 | 10.5564/mjc.v17i43.744 | |||||||||||
日本十進分類法 | ||||||||||||
主題Scheme | NDC | |||||||||||
主題 | 464 | |||||||||||
ISSN | ||||||||||||
収録物識別子タイプ | PISSN | |||||||||||
収録物識別子 | 2226-6739 | |||||||||||
ISSN | ||||||||||||
収録物識別子タイプ | EISSN | |||||||||||
収録物識別子 | 2414-0082 | |||||||||||
著者版フラグ | ||||||||||||
出版タイプ | VoR | |||||||||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||||||||
フォーマット | ||||||||||||
内容記述タイプ | Other | |||||||||||
内容記述 | application/pdf |